Rational construction of hierarchical Ni(OH)(2)-NiS in-plane edge hybrid nanosheet structures on the carbon cloth as a robust catalyst for electro-oxidation of urea

dc.contributor.authorWang, Hui
dc.contributor.authorZhang, Lei
dc.contributor.authorJiang, Huasheng
dc.contributor.authorKannan, Palanisamy
dc.contributor.authorWang, Rongfang
dc.contributor.authorSubramanian, Palaniappan
dc.contributor.authorJi, Shan
dc.date.accessioned2021-10-25T10:00:27Z
dc.date.available2021-10-25T10:00:27Z
dc.date.issued2021
dc.description.abstract-translatedUrea, a non-toxic nitrogenous small molecule, is used for electrochemical energy storage and conversion. However, slow kinetics of urea electro-oxidation reaction and finding an optimal catalyst continues to be major challenges. In this study, we report the preparation of hierarchical Ni(OH)2–NiS in-plane edge hybrid nanosheets on the carbon cloth surface (Ni(OH)2–NiS-CC) as a flexible catalytic electrode by hydrothermal and electroplating processes. The Ni(OH)2–NiS-CC substrate is characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and electro-chemical methods. The developed hierarchical Ni(OH)2–NiS-CC nanosheets electrode shows an enhanced electrocatalytic performance (low-onset oxidation potential, rapid reaction kinetics, and higher mass activity) towards urea electro-oxidation than NiS-CC in an alkaline solution. Counting the benefits including superior catalytic activity, conductivity and available more active sites, the hierarchical Ni(OH)2–NiS-CC in-plane edge hybrid nanosheets electrode displays urea electro-oxidation with a catalytic current of 87.5 mA at 0.8 V vs. Ag/AgCl, which denotes the remarkable electrocatalytic activity as compared with other Ni based catalysts. This simple and useful electrode fabrication method enables a new route to acquire ultra-fine heterostructured substrates for wide variety of potential applications including direct-urea-fuel-cells (DUFC) and urea-assisted water splitting.en
dc.format11 s.cs
dc.format.mimetypeapplication/pdf
dc.identifier.citationWANG, H. ZHANG, L. JIANG, H. KANNAN, P. WANG, R. SUBRAMANIAN, P. JI, S. Rational construction of hierarchical Ni(OH)(2)-NiS in-plane edge hybrid nanosheet structures on the carbon cloth as a robust catalyst for electro-oxidation of urea. JOURNAL OF ALLOYS AND COMPOUNDS, 2021, roč. 87, č. JUL 25 2021, s. nestránkováno. ISSN: 0925-8388cs
dc.identifier.document-number641325500001
dc.identifier.doi10.1016/j.jallcom.2021.159486
dc.identifier.issn0925-8388
dc.identifier.obd43933523
dc.identifier.uri2-s2.0-85102879252
dc.identifier.urihttp://hdl.handle.net/11025/45540
dc.language.isoenen
dc.publisherElsevieren
dc.relation.ispartofseriesJournal Of Alloys And Compoundsen
dc.rightsPlný text je přístupný v rámci univerzity přihlášeným uživatelům.cs
dc.rights© Elsevieren
dc.rights.accessrestrictedAccessen
dc.subject.translatedHybrid nanosheet arraysen
dc.subject.translatedFlexible carbon cloth electrodeen
dc.subject.translatedUrea electro-oxidationen
dc.subject.translatedElectrocatalysten
dc.titleRational construction of hierarchical Ni(OH)(2)-NiS in-plane edge hybrid nanosheet structures on the carbon cloth as a robust catalyst for electro-oxidation of ureaen
dc.typečlánekcs
dc.typearticleen
dc.type.statusPeer-revieweden
dc.type.versionpublishedVersionen

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